苍艾香薰油的气相色谱——质谱分析
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云南中医学院,云南昆明650500

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R2842

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基金项目:云南省应用基础研究项目(NO:2008ZC099M)


An Analysis of Cang-ai Aromatherapy Oils by Gas Chromatography and Mass Spectrometry
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Yunnan University of TCM,Kunming Yunnan 650500

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    摘要:

    目的:研究苍艾香熏油的主要化学成分,考察提取工艺的可行性。方法:采用水蒸气蒸馏法从苍艾复方中提取挥发油,观察苍艾香薰油的稳定性并用气相色谱-质谱联用(GC-MS)法对其主要化学成分进行分析鉴定,用归一法计算各组分的相对百分含量。结果:本实验提取出的挥发油共检测出37种化学成分,鉴定了其中13种主要化学成分及含量,能较好的保留组方中药物的主要成分;高温加热后苍艾香薰油的体积无明显变化,颜色变化较为明显,且对药物化学成分的含量有一定的影响,能降低其大部分有效成分的含量。结论:苍艾香薰油提取工艺可行,能较好的保留组方中药物的主要有效成分。

    Abstract:

    Objective:To analyze the main chemical components of Cang-ai aromatherapy oils and evaluate the feasibility of the extracting technology.Methods:The volatile oils were extracted from the compound Cang-ai by steam distillation.The stability of extraction was observed and the main chemical components were analyzed by gas chromatography and mass spectrometry(GC-MS)as well.The relative percentages of components were counted by normalization calculate.Results:37 chemical components were detected from the volatile extraction and 13 of them were identified the chemical composition which keep the main effective component of the prescription.The volume of Cang-Ai essential oils had no significant change after heatting at high temperature while its color was obviously change.And,the contents of the chemical composition were reduced certainly by heatting.Conclusion:The extracting technology for Cang-ai aromatherapy oils could keep the main effective components of the prescription.

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